Effect of Different Surface Treatments on Shear Bond Strength of Alumina Plate Bonded with Resin Cement

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Techit Subsomboon
Nontapat Hemwutiphan
Nattida Suphatarkul
Nichapa Lomklang
Pemika Lertratanawong
Supichaya Choosuk
Thanapat Sastraruji
Apichai Yavirach
Wissanee Jia-mahasap
Piriya Yavirach
Pisaisit Chaijareenont

Abstract

This study compared shear bond strength of resin cement on different surface treatments of alumina plate. One hundred and thirty rectangular alumina plates were fabricated in size of 10x10x1 mm. Randomly divided alumina plate into ten groups by types of surface treatment: Group 1: Control, Group 2: Sandblast with 50 micron particle pressure 4 bar for 20 seconds, Group 3: Sandblast with 110 micron particle pressure 2 bar for 21 seconds, Group 4: Acid etch with 48% Hydrofluoric, Group 5: Acid etch with Piranha solution, Group 6: Sandblast with 50 micron particle following with 48% hydrofluoric, Group 7: Sandblast with 110 micron particle following with 48% hydrofluoric, Group 8: Sandblast with 50 micron particle following with Piranha’s solution, Group 9: Sandblast with 110 micron particle following with Piranha solution, Group 10 : applied with silane coupling agent. Eight specimens of each group were bonded with RelyX U200 resin cement and evaluated for shear bond strength at cross head speed 0.5 mm/min with universal testing machine. Other three specimens were measured surface roughness with profilometer under testing condition according to ISO4287:1997 with cut off level at 0.8 millimeters and test length of 5 millimeters. Statistical analysis of the mean shear bond strength and surface roughness parameter were analyzed by one-way ANOVA. Last two specimens of each group were observed using scanning electron microscope for surface topography. This study found that surface abrasion with 50-micron alumina particle had highest mean shear bond strength (P<0.05) which related to highest roughness average parameter (P<0.05) and increased in irregular of surface topography from scanning electron microscope. In conclusion, various alumina surface treatment methods affected the mean shear bond strength. Alumina plate abraded with 50-micron abrasive alumina particle had the highest mean shear bond strength and surface roughness.

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Subsomboon T, Hemwutiphan N, Suphatarkul N, Lomklang N, Lertratanawong P, Choosuk S, Sastraruji T, Yavirach A, Jia-mahasap W, Yavirach P, Chaijareenont P. Effect of Different Surface Treatments on Shear Bond Strength of Alumina Plate Bonded with Resin Cement. Khon Kaen Dent J [Internet]. 2018 Dec. 28 [cited 2024 Nov. 20];21(2):94-106. Available from: https://he01.tci-thaijo.org/index.php/KDJ/article/view/163056
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